钻井液用润滑封堵剂的制备与现场应用
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国家重点研发计划“井筒稳定性闭环响应机制与智能调控方法”(项目编号 2019YFA0708303),中国石化科技部“环境响应自 适应封堵防塌钻井液体系研究”(项目编号 P24236)


Preparation and Field Application of a Lubricating and Plugging Agent for Drilling Fluids
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    摘要:

    针对页岩油气经济勘探开发需求,本文对通过对处理剂进行优化设计,以Y#沥青、石油树脂、油溶性酚醛树脂等组合物作为油相基体材料,以氧化石墨烯作为接枝粒子,X#白油作为分散相,并利用有机硅改性剂和有机胺改性剂进行改性,研发出适用于 80~120 ℃易发生井壁失稳井段的润滑封堵剂 SMLP-1,通过对 SMLP-1进行钻井液性能评价分析 SMLP-1 在钻井液体系中的润滑封堵作用及对钻井液性能的影响,通过扫描电子显微镜(SEM)、红外光谱、热重等表征手段证明SMLP-1的作用机理,并进行了现场试验。结果表明,SMLP-1在钻井液中分散性良好,在体系中形成稳定的水包油油滴;加入SMLP-1后,基浆的API滤失量变化不大,但高温高压滤失量明显降低,SMLP-1对降低高温高压滤失量有较强的作用。加入1% SMLP-1后,在常温下润滑系数降低率为16%,150 ℃热滚16后h后润滑系数降低率为43%。SMLP-1可有效封堵泥页岩孔隙,并具有良好的防水侵作用,对膨润土的水化分散具有明显的抑制作用。SMLP-1 成功在溱页 MN03HF 井进行现场试验,累计进尺超过1000 m,加入 SMLP-1后高温高压滤失量由 13.2 mL降至8.6 mL,润滑系数降低率为 30%,不仅减少了钻井液中自由水侵入地层,提高钻井液的封堵能力、稳定井壁,还提高了钻井液的润滑性,保障了复杂井段钻井安全,取得了良好的应用效果。

    Abstract:

    In response to the economic exploration and development needs of shale oil and gas,a lubricating and plugging agent SMLP-1,suitable for 80 —120 ℃ well sections prone to wellbore instability,was developed using Y # asphalt,petroleum resin, oil-soluble phenolic resin and other compositions as the oil phase matrix material,graphene oxide as the grafting particle,X# white oil as the dispersed phase,and using silicone modifier and organic amine modifier to modify. The lubricating and plugging effect of SMLP-1 in the drilling fluid system and its impact on drilling fluid performance were evaluated through the analysis of drilling fluid performance. The action mechanism of SMLP-1 was demonstrated through characterization methods such as scanning electron microscopy(SEM),infrared spectroscopy,and thermogravimetric analysis,and field tests were conducted. The results showed that SMLP-1 had good dispersibility in the drilling fluid,forming stable oil-in-water droplets in the system. After adding SMLP-1, the API filtration loss of the base fluid did not change significantly,but the high-temperature and high-pressure filtration loss was significantly reduced,indicating that SMLP-1 had a strong effect on reducing high-temperature and high-pressure filtration loss. After adding 1% SMLP-1,the lubrication coefficient decreased by 16% at room temperature,and after 16 hours of hot rolling at 150 ℃,the lubrication coefficient decreased by 43%. SMLP-1 could effectively plug shale pores and had good waterproofing and anti-water invasion effects,with significant inhibition on the hydration and dispersion of bentonite. SMLP-1 had been successfully tested on-site in the Qinye MN03HF well,with a cumulative footage exceeding 1000 m. After the addition of SMLP-1,the high-temperature and high-pressure filtration loss decreased from 13.2 mL to 8.6 mL,and the lubrication coefficient reduction rate was 30%. This not only reduced the intrusion of free water into the formation from the drilling fluid,improved the plugging ability and wellbore stability of the drilling fluid,but also enhanced the lubricity of the drilling fluid,ensuring safe drilling in complex well sections and achieving good application results.

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张博文,孔 勇,聂育志,叶清柠,杨安冉,林永学.钻井液用润滑封堵剂的制备与现场应用[J].油田化学,2025,42(4):577-583.
ZHANG Bowen, KONG Yong, NIE Yuzhi, YE Qingning, YANG Anran, LIN Yongxue. Preparation and Field Application of a Lubricating and Plugging Agent for Drilling Fluids[J]. OILFIELD CHEMISTRY,2025,42(4):577-583.

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  • 在线发布日期: 2026-01-28
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