Preparation and Performance Evaluation of Helper-breaking Capsule Type Shielding Temporary Plugging Protection Agent in Fracturing
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    Abstract:

    In order to reduce the damage to the reservoir caused by the leakage of fracturing fluid and the solid phase residue after breaking the gel,based on the shielding temporary plugging oil and gas layer protection theory and the characteristics of microcapsule breaker,the helper-breaking capsule type shielding temporary plugging protection agent in fracturing named TD-1was prepared by liquid drying method,which used organic acid as the core material,ethyl cellulose as the capsule material,polyethylene pyrrolidone as the porogen,and polyvinyl alcohol as the protective agent. The preparation condition was optimized and the performance of TD-1 was evaluated. The results showed that the main particle size of TD-1 was about 300 μm,the content of organic acid in coated core material was 34.1%,and the release rate was 69.0%,when TD-1 was synthesized under the condition of 2.0% polyvinyl alcohol,4.0% ethyl cellulose and polyvinyl pyrrolidone,and 500 r/min stirring rate. TD-1 was helpful for gel breaking of fracturing fluid,which could reduce the viscosity of fracturing fluid by 35.6% and the solid residue content by 44.9%. Meanwhile TD-1 had little effect on the viscosity of fracturing fluid and gel breaking time. TD-1 could form a temporary plugging zone on the surface of reservoir,which could reduce the invasion damage caused by the fracturing fluid filtrate and solid phase material. TD-1 improved the permeability recovery rate by 11.32% and made the core permeability recovery rate reached 82.47%,showing good effect on temporary shield plugging reservoir.

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ZHANG Rusheng, WANG Zengbao, ZHAO Mengyun, LIU Changyin, SUN Zhiyu, JI Yuan, ZHAO Xiutai. Preparation and Performance Evaluation of Helper-breaking Capsule Type Shielding Temporary Plugging Protection Agent in Fracturing[J]. OILFIELD CHEMISTRY,2019,36(2):225-229.

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  • Online: July 31,2019
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