腰果酚基聚醚酯类破乳剂对海上原油的破乳性能研究
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1.东北石油大学化学化工学院;2.大庆市富杰化工有限公司

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Demulsification performance of cashew phenol-based polyether ester demulsifiers
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School of Chemistry and Chemical Engineering,Northeast Petroleum University

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    摘要:

    本研究以生物质腰果酚、甲醛为原料,通过缩合反应制备腰果酚醛树脂起始剂,在碳酸钾催化下通过与碳酸乙烯酯的开环聚合,成功开发了一条腰果酚基聚醚酯破乳剂的绿色合成路线,替代了传统的环氧乙烷、环氧丙烷路线。通过红外光谱和核磁共振氢谱证实了目标产物的化学结构,破乳性能评价显示该破乳剂在加量200 mg/L、70 ℃条件下处理2 h,脱水率高达92.25 %。该研究为开发环保高效的原油破乳剂提供了新思路,拓展了腰果酚在高附加值精细化学品领域的应用。

    Abstract:

    To develop a green synthesis route for cashew phenol-based polyether ester demulsifiers, replacing the traditional ethylene oxide and propylene oxide routes. Biomass cashew phenol and formaldehyde were used as raw materials to prepare cashew phenol aldehyde resin initiators via condensation reaction. Then, ring-opening polymerization with ethylene carbonate was conducted under the catalysis of potassium carbonate. The chemical structure of the target product was confirmed by infrared spectroscopy and 1H NMR. The demulsification performance evaluation showed that under the conditions of a demulsifier dosage of 200 mg/L, 70 ℃, and 2 h, the dehydration rate reached up to 92.25%. This study provides a new idea for the development of environmentally friendly and efficient crude oil demulsifiers, and expands the application of cashew phenol in the field of high value-added fine chemicals.

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  • 收稿日期: 2026-03-12
  • 最后修改日期: 2026-04-25
  • 录用日期: 2026-06-01
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