液体纤维与树脂胶液协同作用对固井水泥浆力学性能的影响
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国家自然科学基金青年基金 “ 基于数据驱动的深水钻井溢流智能识别与反演解释研究 ” (项目编号 51904034),非常规油气省 部共建协同创新中心开放课题 “ 页岩气压裂井井筒重建二次固井环空密封完整性保障方法研究 ” (项目编号 UOG 2024 - 14)。


Synergistic Effect of Liquid Fibers and Resin Binder on Mechanical Properties of Cementing Slurry
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    摘要:

    固井水泥石属于天然脆性材料,水泥环发生破裂会直接引发环空密封失效。为避免水泥石在外载荷冲击 作用下发生破坏,本文将 1 mm 碳纤维与 0 . 7 mm 碳纤维按 4 ∶ 1 比例混合后进行液化分散处理,制备出分散性良 好、可均匀分散于水泥浆的液体纤维;同时对环氧树脂进行改性,得到可改善柔韧性、分散应力的树脂胶液,通过 室内实验探究液体纤维与树脂胶液的协同作用对水泥石力学性能的影响。研究结果表明:当液体纤维加量为 1 %、树脂胶液加量为 3 % 时,水泥浆流变性能良好,失水量小于 40 mL,可满足现场施工的稠化要求,所制备水泥 石的力学性能优于普通水泥石,以及单掺液体纤维或单掺树脂胶液弹韧材料的水泥石。水泥石养护 14 d 后,抗 压强度达 43 . 2 MPa,抗折强度达 14 . 1 MPa,抗冲击强度达 2 . 39 kJ/m2;与普通水泥石相比,弹性极限应变提高 93 . 2 %,弹性模量降低 74 . 2 %,弹性改善效果十分显著。掺入的液体纤维与树脂胶液对水泥石具有良好的增强增 韧效果,可保障外载荷作用环境固井水泥环的长效封隔密封性,提升水泥石抗冲击破坏能力。

    Abstract:

    Cement stone is a natural brittle material. If the cement sheath is broken,it will lead to sealing failure. In order to prevent the cement stone from being destroyed under the impact of external load,the carbon fiber mixture (1 mm carbon fiber and 0 . 7 mm carbon fiber at a mass ratio of 4 ∶ 1) that could be uniformly dispersed in cement slurry,was liquefied and dispersed to obtain liquid fiber with good dispersibility. Epoxy resin was modified to obtain resin emulsion that could improve flexibility and disperse stress. The synergistic effect of liquid fiber and resin emulsion on the mechanical properties of cement stone was studied in laboratory. The results showed that when the dosage of liquid fiber was 1 % and the dosage of resin emulsion was 3 %,the rheological property of the cement slurry was good,and the water loss was less than 40 mL,which could meet the thickening requirements of on-site construction. The mechanical properties of the formed cement stone were better than those of ordinary cement stone,and cement stone doped with single liquid fiber or single resin emulsion elastic-tough material. After 14 days of curing,the compressive strength of the cement stone was 43 . 2 MPa,the flexural strength was 14 . 1 MPa,and the impact strength reached up to 2 . 39 kJ/m2 after 14 days of curing. Compared with common cement stone,the elastic limit strain was increased by 93 . 2 %,and the elastic modulus was decreased by 74 . 2 %,indicating that the elasticity of cement stone was improved obviously. The doped liquid fiber and resin emulsion had a good strengthening and toughening effect on cement stone,which ensured the long-term sealing performance of the cement sheath under external load environment and improved the impact resistance of cement stone.

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王 伟.液体纤维与树脂胶液协同作用对固井水泥浆力学性能的影响[J].油田化学,2026,43(2):191-197.
WANG Wei. Synergistic Effect of Liquid Fibers and Resin Binder on Mechanical Properties of Cementing Slurry[J]. OILFIELD CHEMISTRY,2026,43(2):191-197.

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